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Ti2AlNb热轧板中反常轧制组织成因分析

Mechanism of abnormal rolling microstructure in Ti2AlNb alloy hot-rolled plate

  • 摘要: 本文针对Ti2AlNb热轧板热处理后的组织呈现出的反常取向分层状态进行了分析。利用扫描电子显微镜(SEM)和电子背散射衍射(EBSD)对热轧态和热处理态样品的组织进行了表征,发现热轧态样品内低温平衡相的O相比例高于60%,呈现了类似再结晶的近等轴组织,且大部分β相与O相符合110β∥001O、< 111> β∥< 1-10> O的取向关系。而后继续高温热处理,使得O相向高温β相转变,快冷保留了高温β相,β相呈现明显取向分层现象。热处理前后β相的织构类型未发生明显变化,表明高温β相的形成是热轧态样品中的已有β相晶粒在高温下吞噬周围O相晶粒而长大的过程,并因此而导致β相的取向分布状态保留到了相变之后,从而呈现出独特的取向分层状态。热轧板中的等轴组织是由于高温β相相变形成,低温O相的强织构是由高温β相强织构继承而来。本结果为Ti2AlNb热轧组织的理解和组织调控提供了基础。

     

    Abstract: This paper analyzes the anomalous orientation delamination state exhibitedby the microstructure of Ti2AlNb hot-rolled plates after heat treatment. The microstructure of samples in both hot-rolled and heat-treated conditions was analyzed using Scanning Electron Microscopy (SEM) and Electron Backscatter Diffraction (EBSD). The hot-rolled plates exhibited a near-equiaxed microstructure similar to recrystallization. Moreover,the proportion of the low-temperature equilibrium phase O-phase exceeded 60%. In the hot-rolled state,the majority of the β-phase and O-phase aligned with the orientation relationship 110β//001O,< 111> β//< 1-10> O. Subsequent high-temperature heat treatment led to the transformation of O-phase to the β-phase,while fast cooling retained the β-phase,resulting in noticeable orientation delamination. The texture type of the β-phase exhibited minimal change before and after heat treatment,indicating that the formation of the high-temperature β-phase involves existing β-phase grains from the hot-rolled state growing by engulfing surrounding O-phase grains at elevated temperatures. Consequently,the orientation distribution state of the β-phase is kept after phase transformation,leading to a distinctive orientation layer state. The equiaxed microstructure in hot-rolled sheets arises from the high-temperature β-phase transition,and the strong texture of the low-temperature O-phase is inherited from the strong texture of the high-temperature β-phase. These result provide a foundation for our understanding of the Ti2AlNb hot-rolled microstructure and insights for microstructure regulation.

     

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